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Naphazoline nitrate

CAS No.: 5144-52-5
Product Name:  Naphazoline nitrate
CAS#5144-52-5
Spec: BP2014
Package: 5kg/drum
Delivery time: in stock for prompt shipment.
Dangerous goods or not: Not
Country of origin: China
INQUIRY
Description
Spec of Naphazoline nitrate :
 
Items Specification Results
Appearance White or almost white crystalline powder Conforms
Appearance of solution Clear and colorless Conforms
solubility sparingly soluble in water, soluble in 96% ethanol Conforms
Identification
a. Melting Point
b. U.V. Absorption
c. I.R.Absorption
d. Colour test
a.167.0-170.0℃
b.UV spectrum exhibits maxima at
270.280.287&291
c.I.R Spectrum of sample must comply
with that of the standard
d.A brown colour is observed
a.167.5-170.0 ℃
b.Complies
c.I.R Spectrum of sample is complying with that of the standard
d.Complies
PH(1%) 5.0-6.5 6.3
Loss on drying ≤ 0.50% 0.16%
Sulfated ash ≤ 0.1% 0.004%
Chlorides 330ppm Complies
Related substances by HPLC Impurity A: NMT 0.5%
Unspecified impurities: NMT 0.1% max
Total Impurity: NMT 1.0%
ND
0.02%
0.10%
Residual solvent Methanol: NMT 3000ppm
Ethyl acetate: NMT5000ppm
Chloroform: NMT60 ppm
ND
ND
ND
Microbiological test TAMC: NMT 100cfu/g
TYMC: NMT 10cfu/g
E-Coli: Absent
Saureus: Absent
Salmonlla: Absent
Ps. Aeruginisa: Absent
<1cfu/g
<1cfu/g
Absent
Absent
Absent
Absent
Assay(By Titrimetry) 99.0%~101.00% on dried basis 99.73%

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